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JOURNALS // Uspekhi Fizicheskikh Nauk // Archive

UFN, 2020 Volume 190, Number 9, Pages 971–994 (Mi ufn6553)

This article is cited in 10 papers

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Precise determination of crystal lattice parameters

V. V. Lider

Federal Scientific Research Center Crystallography and Photonics, Shubnikov Institute for Cristallography, Russian Academy of Sciences, Moscow

Abstract: Precision X-ray methods for absolute and relative determination of crystal lattice parameters (interplanar distances) are described and compared, including the X-ray divergent-beam (Kossel) technique, the Bond method, the Renninger method, the back reflection method, the interference method, and the method of standards. It is shown that for most of the considered methods, a relative accuracy of $\sim 10 ^{-5}-10^{-6}$ for determining the lattice parameters is usually achievable, with the last two methods giving a much greater accuracy, at the level of $\sim 10 ^{-8}-10^{-9}$.

Keywords: X-ray radiation, diffraction, Bragg angle, crystal lattice parameter, interplane distance.

PACS: 06.20.Jr, 07.85.-m, 61.05.cp, 61.50.-f

Received: May 14, 2019
Revised: July 1, 2019
Accepted: July 2, 2019

DOI: 10.3367/UFNr.2019.07.038599


 English version:
Physics–Uspekhi, 2020, 63:9, 907–928

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