Optics and Spectroscopy, 2025 Volume 133, Issue 3,Pages 239–246(Mi os1605)
Proceedings of The XXVIII Annual International Conference "Saratov Fall Meeting 2024", September 23-27, 2024, Saratov, Russia. Advanced materials in optoelectronics, laser physics, and photonics Condensed matter spectroscopy
Effect of internal charging on cathodoluminescence profiling capability: boron-implanted $\beta$-Ga$_2$O$_3$
Abstract:
The effect of sample electrification by an electron beam on the integral intensity of cathodoluminescence and on the shape of the emission spectrum is investigated in the work. For this purpose, using the example of Fe:$\beta$-Ga$_2$O$_3$ implanted with boron, the results of cathodoluminescence measurements are compared for three series of experiments: when the surface of the sample under study was not grounded, grounded, or covered with a conductive grounded film. The studies have shown that even when using a metal film, the accumulation of charge under it can distort the shape of the spectrum. Such a distortion of the spectra during a cathodoluminescence study with depth resolution will lead to an incorrect determination of the defect concentration profiles. Comparison of the spectra sequentially recorded with an increase in the electron beam energy and then with a decrease in energy can be proposed as a quick criterion for assessing the effect of charging on the quality of luminescent center profiling.