This article is cited in 13 papers

Macrocyclization with Participation of ThiyI Radicals: Construction of 18- and 9-Membered Crown Thioethers

E. I. Troyanskii^a, D. V. Demchuk^a, M. I. Lazareva^a, V. V. Samoshin^b, Yu. A. Strelenko^a, G. I. Nikishin<sup>a

a</sup> N.D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, Moscow, Russian Federation
^b Department of Chemistry, University of the Pacific, Stockton, California, USA

Abstract: A one-pot synthesis of crown thioethers, 1,10-dioxa-4,7,13,16-tetrathiacyclooctadecanes and 1-oxa-4,7-dithiacyclononanes, which are the 2:2 and 1:1 cycloadducts of the homolytic macrocyclization of alkynes with 3-oxapentane-1,5-dithiol, has been developed.

Language: English

DOI: 10.1070/MC1992v002n02ABEH000124

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