D. G. Mazhukin, L. B. Volodarsky, L. A. Tikhonova, A. Ya. Tikhonov, “Synthesis of 3,4-Dihydro-1,2-diazete 1,2-Dioxides based on 1,2-Bishydroxylamines and 1,2-Nitroso Oxime”, Mendeleev Commun., 1992, Volume 2, Issue 1,Pages <nobr>29

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Synthesis of 3,4-Dihydro-1,2-diazete 1,2-Dioxides based on 1,2-Bishydroxylamines and 1,2-Nitroso Oxime

D. G. Mazhukin, L. B. Volodarsky, L. A. Tikhonova, A. Ya. Tikhonov

N.N. Vorozhtsov Novosibirsk Institute of Organic Chemistry, Siberian Branch of the Russian Academy of Sciences, Novosibirsk, Russian Federation

Abstract: Oxidation of 1,2-bishydroxylamines having one or two hydroxylamino groups at a secondary carbon atom(s), by sodium hypobromite, leads to 3,4-dihydro-1,2-diazete 1,2-dioxides; treatment of 1,2-nitroso oxime with nitric acid or N₂O₄ gives 3,4-dihydro-3-nitro-1,2-diazete 1,2-dioxide.

Language: English

DOI: 10.1070/MC1992v002n01ABEH000111