This article is cited in 11 papers

Hexacyanocyclopropane. Synthesis and Structure

V. M. Anisimov^a, A. B. Zolotoi^b, M. Yu. Antipin^c, P. M. Lukin^d, O. E. Nasakin^d, Yu. T. Struchkov<sup>c

a</sup> N.N. Semenov Federal Research Center for Chemical Physics, Russian Academy of Sciences, Moscow, Russian Federation
^b Institute of Problems of Chemical Physics, Russian Academy of Sciences, Chernogolovka, Moscow Region, Russian Federation
^c A.N. Nesmeyanov Institute of Organoelement Compounds of Russian Academy of Sciences, Moscow, Russian Federation
^d Department of Chemistry, I.N. Ulyanov Chuvash State University, Cheboksary, Russian Federation

Abstract: The synthesis of hexacyanocyclopropane (HCCP) 8 has been carried out for the first time by reaction of tetracyanoethylene 1 with tert-butyl hypochlorite 5 in a water–l,4-dioxane system. The structure of HCCP has been determined by a single crystal X-ray diffraction study of an HCCP·3(l,4-dioxane) adduct.

Language: English

DOI: 10.1070/MC1992v002n01ABEH000107

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