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JOURNALS // Mendeleev Communications // Archive

Mendeleev Commun., 1999 Volume 9, Issue 4, Pages 151–154 (Mi mendc4570)

This article is cited in 4 papers

3,7-Dimethyl-3,7-diazabicyclo[3.3.1]nonane-2,6-dione-1,5-dicarboxylic acid derivatives: synthesis, structure and resolution

R. G. Kostyanovskya, K. A. Lyssenkob, D. A. Lenevc, Yu. I. El'natanova, O. N. Krutiusa, I. A. Bronzovaa

a N.N. Semenov Federal Research Center for Chemical Physics, Russian Academy of Sciences, Moscow, Russian Federation
b A.N. Nesmeyanov Institute of Organoelement Compounds of Russian Academy of Sciences, Moscow, Russian Federation
c Higher Chemical College of the Russian Academy of Sciences, D.I. Mendeleev University of Chemical Technology of Russia, Moscow, Russian Federation

Abstract: Diamide monohydrate 6 was found to form a conglomerate (space group P21), and it was spontaneously resolved by crystallization; esters 1 and 2 were optically enriched by classical methods; the above compounds were structurally characterised by NMR spectroscopy and X-ray analysis.

Language: English

DOI: 10.1070/MC1999v009n04ABEH001067



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