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JOURNALS // Fizika Tverdogo Tela // Archive

Fizika Tverdogo Tela, 2022 Volume 64, Issue 10, Pages 1545–1551 (Mi ftt11171)

Phase transitions

Temperature investigations of magnetic properties when analyzing the structural phase state of a model nanocomposite with carbidosteel composition

A. I. Ulyanov, A. A. Chulkina, A. L. Ulyanov

Udmurt Federal Research Center of the Ural Branch of the Russian Academy of Sciences, Izhevsk, Russia

Abstract: The phase composition, magnetic state of the phases and their influence on the formation of the magnetic hysteresis properties of the nanocomposite with the (Fe$_{0.85}$Mn$_{0.10}$Ni$_{0.05}$)$_{83}$C$_{17}$ composition after mechanosynthesis and subsequent annealing have been studied. It is shown that, although the dependences of the coercive force on the annealing temperature $H_c(T_{\text{ann}})$ of the alloy, measured at room and liquid nitrogen temperatures, are curves with maxima, the formation of $H_c$ is driven by different mechanisms. At room temperature measurements, the maximum $H_c$ value of the composite is obtained when the size of the ferrite phase precipitates approaches to the critical single-domain state, whereas at low temperature maximum $H_c$ value is caused by the change of the cementite structural state upon annealing.

Keywords: nanocrystalline Fe–C–Mn–Ni alloys, mechanical alloying, heat treatment, X-Ray diffraction, coercive force, magnetic susceptibility, Curie temperature, Mössbauer spectroscopy.

Received: 17.05.2022
Revised: 17.05.2022
Accepted: 22.05.2022

DOI: 10.21883/FTT.2022.10.53104.381



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